The chemical industry reduces the impact on the environment during synthesis 627-42-9, name is 2-Methoxyethyl chloride, I believe this compound will play a more active role in future production and life. 627-42-9
To a solution of 3,4-dihydroxybenzaldehyde (10 g, 72.5 mmol) (Aldrich) in DMF (200 mL) was added 2-chloroethyl methyl ether (16.5 mL, 181.2 mmol) (Aldrich), potassium carbonate (50 g, 362.3 mmol) and a catalytic amount of potassium iodide (Aldrich). The reaction mixture was heated at 85 C. for 14 hours. The reaction mixture was cooled down, diluted with EtOAc and washed with brine. The organic phase was dried over anhydrous sodium sulfate, evaporated to afford 3,4-bis-(2-methoxy-ethoxy)-benzaldehyde as an oil and was used in the next step without further purification. (Yield 11 g, 70%).
The chemical industry reduces the impact on the environment during synthesis 627-42-9. I believe this compound will play a more active role in future production and life.
Reference:
Patent; Dominique, Romyr; Luk, Kin-Chun; Qiao, Qi; Rossman, Pamela Loreen; US2012/184548; (2012); A1;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics