In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 39226-95-4 as follows. SDS of cas: 39226-95-4
General procedure: Amine (0.386 mL) was added to Triton-B and stirred for 10 min followed by the addition of CS2 (0.321 mL) dropwise. Then dimethyl acetate carboxylate was added again dropwise. The mixture was stirred for 2.5 h. TLC plate showed the formation of some new compound. The reaction was seen continuously and formation of product was monitored with TLC. After the completion, the reaction mixture was drained into distilled water and extraction was done three times using ethyl acetate (Scheme-I)
According to the analysis of related databases, 39226-95-4, the application of this compound in the production field has become more and more popular.
Reference:
Article; Srivastava, Nitin; Saxena; Asian Journal of Chemistry; vol. 31; 1; (2019); p. 176 – 180;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics