Adding a certain compound to certain chemical reactions, such as: 627-42-9, name is 2-Methoxyethyl chloride, belongs to chlorides-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 627-42-9, Formula: C3H7ClO
1) according to the amount of substance, the 2 portions N-methyl imidazole is added to the round-bottom flask, then adding normal heptane, magnetic stirring, the stirring speed is 500 revolutions/minutes, until the reaction is complete;(2) for the shares N-methyl imidazole 1.1 times of chloroethyl methyl ether is added to the above-mentioned solution; nitrogen protection, the water bath temperature control, magnetic stirring, at a temperature of 80 C reaction under 48 hours;(3) to the upper layer solution retrodisplacement reaction is ended, the lower layer solution is extracted with ethyl acetate 3 times, vacuum distillation to obtain intermediate 1-methyl, 3-methyl ether chloride ion ionic liquid
At the same time, in my other blogs, there are other synthetic methods of this type of compound, 2-Methoxyethyl chloride, and friends who are interested can also refer to it.
Reference:
Patent; Huanghuai College; Feng, Xiantao; Wei, Yu; Zhang, Jingxun; (6 pag.)CN105399679; (2016); A;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics