Application of 622-24-2, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 622-24-2 as follows.
To the reaction flask was added substances five, six substances, dimethylformamide, potassium carbonate, the reaction was cooled to 25 , the reaction mixture was added to ice water, ice-water is 10 times the mass of the reaction liquid was filtered, washed with water, Dry matter seven. The molar ratio of the substance five, substance six, potassium carbonate and dimethylformamide was 1: 1: 1: 10, and the temperature was raised to 80 C for 4 hours
According to the analysis of related databases, 622-24-2, the application of this compound in the production field has become more and more popular.
Reference:
Patent; CHINA THREE GORGES UNIVERSITY; TAN, XIAO; LIU, SEN; YANG, LITING; (22 pag.)CN106243058; (2016); A;,
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