Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 112-26-5, name is 1,2-Bis(2-chloroethoxy)ethane, A new synthetic method of this compound is introduced below., Formula: C6H12Cl2O2
Potassium carbonate (11.0g, 79.3mmol) in the presence of, at 50 , 4- hydroxythiophenol (1e) (10.0g, 79.3mmol) and 1,2-bis (chloroethoxy) ethane ( the reaction 7.06g, 37.76mmol) in place in DMAc35ml. using ethyl acetate / water system after the separating operation was performed to obtain crystals of the diol was purified by column (2b) (5.7g, 42%).
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; Fuji Photo Film Co., Ltd.; Song, Shantashi; Jia, tengjunye; (56 pag.)CN104159996; (2016); B;,
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