Related Products of 1005-56-7, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 1005-56-7, name is O-Phenyl carbonochloridothioate belongs to chlorides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
(Scheme 5) 438.5 mg (1.0 mmol) of a rhodamine compound (for example, a synthetic product of 1,6-dihydroxy naphthalene and 4-diethylamino keto acid),690.4 mg (4.0 mmol) phenyl thiochloroformate and (350 muL)N,N-diisopropylethylamine(DIPEA) dissolved in 15 mL of dichloromethane,Then stir at room temperature for 15h,After vortexing to obtain a crude product,Finally using dichloromethane:Column chromatographic separation of the methanol system (30:1, v/v)506 mg of pure product was obtained with a yield of 88%.
The synthetic route of O-Phenyl carbonochloridothioate has been constantly updated, and we look forward to future research findings.
Reference:
Patent; University of Jinan; Zhang Meng; Wu Liu; Zhao Ziyang; Yuan Ruifang; Fang Zhaotong; Wang Ruikang; Liu Caiyun; Zhu Baocun; (11 pag.)CN107903237; (2018); A;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics