Related Products of 38762-41-3, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 38762-41-3, name is 4-Bromo-2-chloroaniline belongs to chlorides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
General procedure: A 25 mL RBF was subsequently charged with 1.0 mmol aromatic amines, 1.0 mmol 4-hydroxybutan-2-one, 10 mol% I2 (25.4 mg), 2mL DMSO. The resulting mixture was performed at room temperature for 8 h. After reaction was complete, the resulting mixturewas poured into water (20 mL) and extracted with ethyl acetate (3 x10 mL). The combined organic extracts were washed with brine (3 5 mL), then dried over Na2SO4 and concentrated in vacuum. The resulting residue was purified by silica gel columnchromatography (ethyl acetate/petroleum ether 1:20-1:4) to afford the desired products.
The synthetic route of 4-Bromo-2-chloroaniline has been constantly updated, and we look forward to future research findings.
Reference:
Article; Miao, Changqing; Jiang, Liya; Ren, Lanhui; Xue, Qingxia; Yan, Fang; Shi, Weiwei; Li, Xinjian; Sheng, Jiwen; Kai, Shuangshuang; Tetrahedron; vol. 75; 14; (2019); p. 2215 – 2228;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics