Electric Literature of 870-24-6, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 870-24-6, name is 2-Chloroethanamine hydrochloride belongs to chlorides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Step 3: Synthesis of t-butyl (2-chloroethyl)carbamate: 28.7 g (249 mmol) of 2-chloroethylamine hydrochloride was dissolved in 300 ml of dichloromethane. 41 g (192 mmol) of di-t-butyl dicarbonate and 80 ml (576 mmol) of triethylamine were added to the obtained solution, and they were stirred overnight. After the treatmentwith dichloromethane as the extraction solvent in an ordinary manner, the title compound was obtained. Yield: 41 g (229 mmol) (92 %) H-NMR (CDCl3) delta 1.43 (9H, s), 3.41 (2H, dt), 3.59 (2H, t), 4.95 (1H, br)
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 2-Chloroethanamine hydrochloride, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Ajinomoto Co., Inc.; EP1065200; (2001); A1;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics