Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 13078-79-0, name is 2-(3-Chlorophenyl)ethanamine, A new synthetic method of this compound is introduced below., Product Details of 13078-79-0
General procedure: NaBH(OAc)3 (3 eq) was added to an ethanol solution (15 mL)of the aldehyde 9 (1 g) and alkylamines (2 eq), and the mixture was stirred for 4 h at 0 to room temperature. After completionof the reaction, the reaction mixture was evaporated under reduced pressure to give a crude residue, which was purified by asilica gel (300-400 mesh) column using petroleum ether/ethyl acetate (5:1?2:1) to obtain pure compound 10a-i.
The synthetic route of 13078-79-0 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Wang, Haibo; Pan, Yang; Tang, Qin; Zou, Wei; Shao, Huawu; Chinese Chemical Letters; vol. 29; 1; (2018); p. 73 – 75;,
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