Application In Synthesis of 1-Chloro-2-methylbenzene. In 2019.0 RSC ADV published article about ONE-POT SYNTHESIS; RUTHENIUM-CATALYZED AMINATION; HETEROCYCLIZATION SYNTHESIS; DEHYDROGENATIVE SYNTHESIS; NITROGEN-HETEROCYCLES; 3-COMPONENT SYNTHESIS; BORROWING HYDROGEN; DERIVATIVES; EFFICIENT; ALDEHYDES in [Debnath, Pradip] Maharaja Bir Bikram Coll, Dept Chem, Agartala 799004, Tripura, India in 2019.0, Cited 91.0. The Name is 1-Chloro-2-methylbenzene. Through research, I have a further understanding and discovery of 95-49-8.
An efficient and operationally simple protocol has been demonstrated for the synthesis of 1,3,5,7-tetrasubstituted pyrimido[4,5-d]pyrimidines via TBHP-mediated direct oxidative coupling of N-uracil amidines and methylarenes under metal-free conditions. Due to the inherent stability of methylarenes compared to aldehydes, the presented synthetic protocol is adaptable to a broad substrate scope, is operationally simple, has no need for stringent protection in the whole preparation process, and has the potential to prepare valuable products that are currently inaccessible or challenging to prepare using conventional methods. It is a significantly important complement to the conventional synthetic methods. The reaction possesses an efficient tandem oxidation-imination-cyclization process.
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Reference:
Patent; Nanjing Zhongteng Chemical Co., Ltd.; Zhong Hua; Lu Minshan; Chen Xiuzhen; Liu Qiaobao; Yin Hengbo; Wang Aili; (8 pag.)CN104876790; (2017); B;,
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