Bailey, William J. published the artcilePyrolysis of esters. XXII. Synthesis of bisdienes from 2-hydroxymethyl-1,3-butadiene, Quality Control of 866-23-9, the publication is Journal of Organic Chemistry (1962), 2732-6, database is CAplus.
cf. CA 57, 4529d. A new synthesis of 2-hydroxymethyl-1,3-butadiene was developed, starting from commercially available 2-amino-2-ethyl-1,3-propanediol and involving a pyrolysis of an amine oxide as well as the pyrolysis of an ester. Hydroxymethylbutadiene treated with vinyl acetate in the presence of a mercuric oxide-boron trifluoride etherate mixture gave 38% bis(2-butadienylmethyl) acetal. Treatment of the hydroxymethylbutadiene with hexamethylene diisocyanate gave 76% solid bis(2-butadienylmethyl) hexamethylenecarbamate, while treatment with m-xylylene diisocyanate gave 91% solid bis(2-butadienylmethyl) m-xylylenecarbamate.
Journal of Organic Chemistry published new progress about 866-23-9. 866-23-9 belongs to chlorides-buliding-blocks, auxiliary class Aliphatic Chain, name is Diethyltrichloromethylphosphonate, and the molecular formula is C5H10Cl3O3P, Quality Control of 866-23-9.
Referemce:
https://en.wikipedia.org/wiki/Chloride,
Chlorides – an overview | ScienceDirect Topics