Lai, J. S.’s team published research in Journal of Organometallic Chemistry in 393 | CAS: 5034-06-0

Journal of Organometallic Chemistry published new progress about 5034-06-0. 5034-06-0 belongs to chlorides-buliding-blocks, auxiliary class Salt,Aliphatic hydrocarbon chain, name is trimethyloxosulphonium chloride, and the molecular formula is C3H9ClOS, Application of trimethyloxosulphonium chloride.

Lai, J. S. published the artcilePreparation of sulfur ylide complexes of platinum by phase transfer catalysis, Application of trimethyloxosulphonium chloride, the publication is Journal of Organometallic Chemistry (1990), 393(3), 431-40, database is CAplus.

Various sulfur ylide complexes of Pt were prepared by the phase transfer catalysis (PTC). Thus, reaction of Pt(PR3)2Cl2 (R = Me, Ph) in CH2Cl2 with [S(O)(CH3)3]I under PTC/OH conditions give complexes {Pt(PR3)2[(CH2)2S(O)(CH3)]}I, which contain a bidentate double sulfur ylide. With Pt(dppe)Cl2 [dppe = Ph2P(CH2)2PPh2] as starting material, a similar product was obtained. But when Pt(dppm)Cl2 [dppm = Ph2PCH2PPh2] was treated with [S(O)(CH3)3]Cl under PTC/OH conditions, an unexpected product {Pt(PPh2CH3)(PPh2OH)[(CH2)2S(O)(CH3)]}Cl was obtained. This compound contains a bidentate double sulfur ylide and two unsym. phosphines resulting from the base hydrolysis of dppm. Compound {Pt(PPh3)2[(CH2)2S(O)(CH3)]}I, was subjected to an x-ray diffraction study.

Journal of Organometallic Chemistry published new progress about 5034-06-0. 5034-06-0 belongs to chlorides-buliding-blocks, auxiliary class Salt,Aliphatic hydrocarbon chain, name is trimethyloxosulphonium chloride, and the molecular formula is C3H9ClOS, Application of trimethyloxosulphonium chloride.

Referemce:
https://en.wikipedia.org/wiki/Chloride,
Chlorides – an overview | ScienceDirect Topics