Li, Xiao-Juan published the artcileConvenient and efficient decarboxylative aldol reaction of malonic acid half esters with trifluoromethyl ketones, Formula: C8H4ClF3O, the publication is Tetrahedron Letters (2012), 53(16), 2117-2120, database is CAplus.
A convenient and efficient decarboxylative ketone aldol condensation of malonic acid half esters was reported. In the presence of catalytic amount of triethylamine, a series of aromatic and alkyl trifluoromethyl ketones were transformed into the desired adducts in 61-99% yields. In a preliminary experiment, a moderate stereoselectivity was obtained. Direct reduction of the aldol product with LiAlH4 afforded trifluoromethylated 1,3-diol.
Tetrahedron Letters published new progress about 5860-95-7. 5860-95-7 belongs to chlorides-buliding-blocks, auxiliary class Trifluoromethyl,Fluoride,Chloride,Benzene,Ketone, name is 1-(2-Chlorophenyl)-2,2,2-trifluoroethanone, and the molecular formula is C8H4ClF3O, Formula: C8H4ClF3O.
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Chlorides – an overview | ScienceDirect Topics