Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 18487-39-3, name is 2,3,5-Trichloroaniline, A new synthetic method of this compound is introduced below., COA of Formula: C6H4Cl3N
EXAMPLE 11 The procedure of the preceding example is followed, except for the following conditions: A 4 N aqueous solution of HCl (120 cc), 2,3,5-trichloroaniline (0.354 g), a palladium-based catalyst (palladium on carbon activated containing 10% of palladium) (0.140 g) and potassium iodide (0.011 g) are introduced. The autoclave is heated at 160 C. for 160 minutes under a total pressure of 18 bars, the hydrogen pressure being 13 bars. The conversion is complete and 3,5-dichloraniline is obtained with a yield of 96.8%.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; Rhone-Poulenc Agrochimie; US4351959; (1982); A;,
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