Electric Literature of 2687-12-9, A common heterocyclic compound, 2687-12-9, name is Cinnamyl chloride, molecular formula is C9H9Cl, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Specifically, a 200 mL flask containing 15.3 g (0.1mol) of compound lb and 25 g (0.15 mol) of triethyl phos-phite was stirred for 8 hours at 180 C.Next, afier cooling the flask to room temperature, excess triethyl phosphite was evaporated under reduced pressure to yield 22 g (percentage yield: approximately 87%) ofthe compound 3b (white liquid).
The synthetic route of 2687-12-9 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; KYOCERA Document Solutions Inc.; OKADA, Hideki; SUGAI, Fumio; KOJIMA, Kensuke; (23 pag.)US2016/152552; (2016); A1;,
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