Related Products of 3228-99-7, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 3228-99-7, name is Pentaerythrityl Tetrachloride belongs to chlorides-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
General procedure: In the ovenDriedNitrogen gas in a stainless steel high pressure reactor with a capacity of 75 millilitersUnder0.4 g (0.16 mmol)And tributylphosphine immobilized on chloropropyl silsesukuoxen15 g (0.13 mol) of chloroform and 52.8 g(0.39 mol) of trichlorosilane was added. Seal the reactorAfter reacting at 150 for 2 hours, the reactant was distilled under reduced pressure.18.9 g (yield 51.3%) of bis (trichlorosilyl) methane was obtained
The synthetic route of Pentaerythrityl Tetrachloride has been constantly updated, and we look forward to future research findings.
Reference:
Patent; JSI Silicone Co., Ltd.; Jeong Il-nam; Kim Eun-seong; Kim Seong-min; Kim Yeong-min; (13 pag.)KR2020/15644; (2020); A;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics