Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 6626-57-9, name is 1,3-Dichloro-2,2-dimethoxypropane, A new synthetic method of this compound is introduced below., Product Details of 6626-57-9
The last step was dissolved in 125mL solid 42.24g methylene chloride: water = 6: 1 in a mixed solvent, at 20-35 under fed 42.0g chlorine, chlorine was stopped and stirring was continued for 0.5 hours, after standing points the aqueous layer, the organic layer was dried over anhydrous magnesium sulfate, and the solvent evaporated under reduced pressure and the low-boiling by-products, 1,3-dichloro-acetone to give a colorless liquid 30.45 g, 97.7% pure by gas chromatography, a yield of 96.2%
The synthetic route of 6626-57-9 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Southeast University; Wang, MingLiang; Wang, Jia; Dan, hongbin; Gu, xiantao; Wang, shengzhi; Zhang, Wei; (5 pag.)CN105461529; (2016); A;,
Chloride – Wikipedia,
Chlorides – an overview | ScienceDirect Topics