Related Products of 76958-07-1, In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 76958-07-1 as follows.
[00378] N-[(6-chloro-1 ,3-benzodioxol-5-yl)carbamothioyl]benzamideImage available on “Original document”[00379] To 1 .88g ( 0.025 mol) of anhydrous ammonium thiocyanate in 40 ml acetone was added dropwise 3.2 g (0.023 mol) of benzoyl chloride. The resulting mixture was heated to reflux. Heating was removed and a solution of 3.8g (0.022 mol) of the amine in 15 ml dry acetone was added at a rate to maintain the mixture at boiling. After an additional 15 minutes reflux the reaction was cooled and the precipitate was filtered off. The precipitate was washed with acetone and dried to yield 5.5 g of the product.
According to the analysis of related databases, 76958-07-1, the application of this compound in the production field has become more and more popular.
Reference:
Patent; KINEATA INC; Ladonato, Shawn P.; Bedard, Kristin M.; Munoz, Ernesto J.; Imanaka, Myra W.; Fowler, Kerry W.; (122 pag.)WO2014/113492; (2014); A2;,
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